Features | 、Reactor made of Ni-based superalloy, which allows high pressure at high temperature (up to 3MPaat 1100 °C) 、Over-temperature alarm and interlock are installed for safe operation 、Over-pressure alarm is installed. A solenoid valve is installed for automatic pressure relief 、Temperature control andpressuremonitoring software are includedfor remote control |
Structure | 、Please click drawing left to see detail structure 、Warning #1: For your safety, never face on top flange without protective wear. 、Warning #2:The high-pressure vessel and furnace must be placed inside an explosive-proof box or case during using under high pressure. (Please check the images below for some idea . Customized proof is available upon request) |
Input Power | 、Input voltage: 208 - 240 VAC, 50/60 Hz, single phase 、1.5kWpower |
Pressure Vessel | 、Ni-based superalloy hydrothermal reactor with 300 mL capacity. Attention: Processing vessel is consumable, you can click the left picture to order replacement or a spare one 、Made of Ni-based superalloy GH747 (Click to download GH747 nickel based alloy datasheet) 、Reactor size: 70 mm ODx35 mm IDx326 mm H 、Air cooled flange via aluminum heat radiator 、A small quartz or alumina boat should be used to load the sample inside the reactor, which increases vessel service life •Gold or Ni foil can be used to wrap the crucible boat to minimize contamination to the vessel 、It is customer responsibility to find suitable liner for different material for hydrotheral crystal growth. 、Optional torque wrench is availableto avoid overtightening the flange bolts |
Working Pressure | 、16.5 MPa (2393 PSI) ≤ 800 °C 、10 MPa (1450 PSI) ≤ 900 °C 、5 MPa (725 PSI) ≤ 1000 °C 、3 MPa (435 PSI) ≤ 1100 °C |
Pressure Monitoring and Relief | 、Precisionhigh pressuresensor (measurement range up to 25MPa, or 250bar) is installed on the pressure vessel. The pressure monitor displays pressure in bar 、Pressure monitor allows the user to set a high pressure alarm. When the pressure reaches the alarm set point (15 MPa max), alarm will sound and the pressure will be released via a solenoid valve on the flange.For using the reactor with a pressure gt; 15 MPa at low temperature, please shut off the needle valve near the solenoid valve and use the manual pressure relief valve |
Temperature Control amp; Heater | 、Working temperature: 1100 ℃max (< 1 hour). Continuous working temperature: ≤ 1000 °C 、Heating/cooling rates: ≤ 10 °C/min 、Heating zone length: 330 mm 、Constant temperature zone: 80 mm within +/- 1 °C 、Heating element: Fe-Cr-Al alloy 、Thermocouple: K-type(Omega 3 mm OD K Typewith high-temperature tolerance (220°C) connector) 、One digital temperature controller with 30 programmable segments and +/- 1 ºC accuracy |
PC Control (optional) | •MTS-02 |
Accessories | 、SS316 needle valve with 1/4 pipe connector amp; pressure gauge are included 、Twoconsumable Copper Gasket (63 mm OD)are included (Click the left picture to order extra) |
Size | 、340 mm Wx320 mm Dx820 mm H |
Net Weight | 、35 kg |
Warranty | 、One year limited warranty with lifetime support |
Operation Instructions | |
Application Notes | 、The recommended temperature heating/cooling rate is 5~10 ºC/min 、DONOTover tighten the flange screws as this may cause permanent damage to the flange or screws. Please refer tothe instructionabout proper torque for installing CF flange bolts.We recommend youtouse a torque wrench to tighten the screws with the flange 、DO NOT use the pressure relief solenoid valve.to vent the vessel! It could contaminate the valve and impact its service life. Always use the manual pressure relief valve for venting 、Warning: For your safety, the high-pressure vessel must be placed inside an explosive-proof box or case during using under high pressure. Never face on top flange without protection to avoid the accident. 、Please click picture and drawing below left to see detail structure, and click pic right to order an Explosion-Proof Box |
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