High Pressure Tube Furnace with Optional Alloy Tube(900℃or 1100℃max heat temp.)OTF-1200X-HPV-$system.title}

High Pressure Tube Furnace with Optional Alloy Tube(900℃or 1100℃max heat temp.)OTF-1200X-HPV

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High Pressure Tube Furnace with Optional Alloy Tube (900℃ or 1100℃ max heat temp.) - OTF-1200X-HPV

OTF-1200X series high-pressure split tube furnaces can be chosen from two kinds of alloy tube, e.g. Stainless steel 310S refractory alloy or Ni-based superalloy, which offer a solution of heating treatment under high positive pressure with/without inert gas support to process special compound material. The furnace can be heated up to the max. 900℃or 1100℃with the optional vessel. The operating positive pressure is from 105 to 800 psi according to different heating temperature. 、Heating temperature up to max. 900℃or 1100°C, Depends on tube alloy 、Stainless steel or nickel-base superalloy processing tube is included ( please choose from product optional ) 、Max pressure up to 800 PSI.depended on tube alloy 、Double layer steel casing with air cooling to keep furnace surface temperature lower than 60°C. High purity fibrous alumina insulation for Max. energy saving 、PID automatic control with 30 steps programmable. Automatic overtemperature and thermally broken protection 、One set of high positive pressure flange 、The pressure sensor is installed in the flange. The pressure will be displayed in the pressure controller in the front panel of the furnace. The alarm system is built in the pressure controller which allow the user to set up the high and low limit point of pressure. When the measuring pressure exceeds the limit point, the alarm strobe and whistle will be activated for warning 、The furnace is able to be controlled by a computer. And the software and USB cable are included
SPECIFICATIONS
OTF-1200X-HVHP-80(60)-SSOTF-1200X-HVHP-60-GH
Process Vessels (Pls select the tube size in options bar)SS310S Stainless Steel alloy80mm O.Dx70(±2) mm I.Dx1000 mm L or 60mm O.Dx50(±2)x1000 mm LNi-based superalloyGH747 (Click to download GH747 nickel-based alloy datasheet) OD 60xID 52xLength 1000 (mm)
Copper gasketFor 80mm O.D tube:99 O.Dx82 I.Dx2.2mmFor 60mm O.D tube:82 O.Dx63.6 I.Dx2.2mmFor 60mm O.D tube:82 O.Dx63.6 I.Dx2.2mm
Working Pressure vs. Working Temperature 577 PSI max at ≤500℃511 PSI max at ≤600℃428 PSI max at ≤700℃203 PSI max. at ≤800℃116 PSI max at ≤900°CAttention: Never heat up above 900℃900℃max.for < 1hr 580 PSI (4 Mpa) max. at ≤800°C362 PSI (2.5 Mpa) max. at ≤900°C174 PSI (1.2Mpa) max. at ≤1000°C116 PSI (0.8 Mpa) max. at 1100°CAttention: Never heat up above 1100°CThe furnace also can reach high vacuum up to 10-6 torr by turbopump.
Pressure Measurement Range0~15Mpa0~15Mpa
Max. Heating Temperature 900°C1100°C
Working GasesInert gas amp; HydrogenInert gas, hydrogen, and oxygen
Heating Temperature1100℃max.for < 1hr 800℃continuous1100℃max.for < 1hr 1000℃for continuous
Heating Rate≤30°C/min≤20°C/min
Heating ElementFe-Cr-Al Alloy doped by MoFe-Cr-Al Alloy doped by Mo
Heating ZoneTotal length: 440mm Single zoneConstant temp. zone: 150mm ±1°CTotal length: 440mm Single zoneConstant temp. zone: 150mm ±1°C
Temperature Control PID control method with over-temp protectionTemperature stability: ±1°CDemo video here)PID control method with over-temp protectionTemperature stability: ±1°CDemo video here)
ThermocoupleOmega 3mm OD K Typewith high-temperature tolerance (220°C) connectorOmega 3mm OD K Typewith high-temperature tolerance (220°C) connector
Positive Pressure SensorInstalled in high-pressure flangeInstalled in the high-pressure flange
PC Control (Optional)
Pressure Alarm SystemThe upper limit and lower limit control methodAlarm strobe and warning whistleThe upper limit and lower limit control methodAlarm strobe and warning whistle
VoltageAC 220V 50/60HzAC 220V 50/60Hz
Power2.5KW(20A breaker required)2.5KW(20A breaker required)
Application Notes 、The heating temperature must be limited by the certain pressure level due to vessel material strength. Please refer to the specifications 、The pressure increases while the temperature is rising during operation. So you need to calculate the pressure changing towards your target temperature and set a safe value of pressure during the process 、The furnace uses a tube with conflate designed flanges. 、Note: Please never use ordinary SS tube to connect to gas-inlet for using gt; 5Mp pressure, which may cause tube exploded. 、The safety pressure relief valveis available to be installed at the downstream side. Please click here for details. 、A small quartz or Alumina boat should be used to load the sample into the vessel. Please click the link below to order separately. Never place the sample directly onto the vessel without a crucible. Vessel service-life could be reduced significantly if you do so. •You may use gold or nickel foil to wrap the crucible boat to minimize the contamination to the pressure vessel. 、Optional torque wrench is available hereto avoid overtightening the flange bolts 、To measure the electric properties ofthermoelectric ceramics under high pressure amp; temperature conditions, pleaseorder alumina testing fixture and high-pressure electrical feedthrough (10Mpa Max.) with the furnace (additional fee will apply).
Safety Note 、Ni-based Superalloy ( Waspaloy or equivalent) is a reliable processing tube which can be used under high temperature and high pressure. It has excellent ductility and tensile property so only creep deformation happens under overpressure destruction test and following by a crack formed (usually at the hot zone at the center of the tube) to release the pressure. Brittle fracture won’t happen in the overpressure destruction test which means no tube explosion will happen under the overpressure of inert gas or safe gas or under other accidents causing overpressure of inert gas or safe gas. The pics show Ni-based Superalloy tube under overpressure test 、Attention: For the use with flammable, toxic or corrosive gas, you must contact STR-engineering group for the consultation to know all the prerequisites and precautionary measures. 、Attention: A two-stage pressure regulator must be installed on the gas cylinder to limit the pressure to below 3 PSI for safe operation. Please click here to learn how to install the gas regulator. 、Do not over tightening the flange screws as this may cause permanent damages to the flange or screws. Please refer to the instructions about proper torque for installing CF flange bolts. We recommend you use atorque wrenchto tighten the screws with the flange.
Operation Instructions
WarrantyOne-year limited manufacturer warranty with lifetime support (Consumable parts such as processing tubes, o-rings, and halogen lamps are not covered by the warranty, please order replacements at related products below).
STANDARD PACKAGE
P/NNameQtyOTF-1200X-HVHP-60OTF-1200X-HVHP-80OTF1200X-60UV
Tube Furnace main machine1
Processing vessel1SS310S alloy - 60SS310S alloy - 80Ni based alloy-60
High-pressure flange set (1 pair)1
ORing-Cu82Oxygen-free copper gasket3
MTS02USB cable and software for temp management1
FLG-kit-2Furnace hook1
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